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ChemicalBook CAS DataBase List BisdeMethoxycurcuMin
52328-96-8

BisdeMethoxycurcuMin synthesis

3synthesis methods
-

Yield:52328-96-8 88%

Reaction Conditions:

Stage #1: acetylacetonewith boron trioxide in ethyl acetate at 80; for 0.5 h;
Stage #2: 4-hydroxy-benzaldehydewith boric acid tributyl ester in ethyl acetate at 80; for 0.5 h;Further stages;

References:

Di Martino, Rita Maria Concetta;De Simone, Angela;Andrisano, Vincenza;Bisignano, Paola;Bisi, Alessandra;Gobbi, Silvia;Rampa, Angela;Fato, Romana;Bergamini, Christian;Perez, Daniel I.;Martinez, Ana;Bottegoni, Giovanni;Cavalli, Andrea;Belluti, Federica [Journal of Medicinal Chemistry,2016,vol. 59,# 2,p. 531 - 544]