Boc-DL-aspartic acid synthesis

2synthesis methods

24424-99-5 Synthesis

617-45-8 Synthesis

Yield:120341-32-4 98%

Reaction Conditions:

Stage #1: aspartic Acidwith sodium hydroxide in 1,4-dioxane;water; for 0.333333 h;
Stage #2: di-tert-butyl dicarbonate in 1,4-dioxane;water at 25;

References:

Jiang, Min;Yang, Haijun;Fu, Hua [Organic Letters,2016,vol. 18,# 9,p. 1968 - 1971] Location in patent:supporting information

147291-69-8 Synthesis

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