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Boc-TOTA-N3 synthesis

4synthesis methods
4246-51-9 Synthesis
4,7,10-TRIOXA-1,13-TRIDECANEDIAMINE

4246-51-9
169 suppliers
$6.00/5g

Boc-TOTA-N3

1162070-33-8
11 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: dichloromethane / 12 h / 20 °C
2: 1H-imidazole-1-sulfonyl azide hydrochloride; potassium carbonate; copper(ll) sulfate pentahydrate / methanol / 20 °C

References:

Wang, Tao;Ng, David Y. W.;Wu, Yuzhou;Thomas, Jessica;Tamtran, Thuy;Weil, Tanja [Chemical Communications,2014,vol. 50,# 9,p. 1116 - 1118]