Borazine, hexamethyl- synthesis
- Product Name:Borazine, hexamethyl-
- CAS Number:877-07-6
- Molecular formula:C6H18B3N3
- Molecular Weight:164.66
703-86-6
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75-16-1
275 suppliers
$12.00/10ml
1826-67-1
220 suppliers
$60.89/100ml
16898-38-7
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38828-96-5
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877-07-6
5 suppliers
$156.00/250MG
Yield:16898-38-7 63% ，38828-96-5 7% ，877-07-6 16%
Reaction Conditions:
in diethyl ether;N2 atmosphere; addn. of soln. of MeMgBr in Et2O to soln. of B-compd. in Et2O(room temp.), stirring (1 h, room temp.), addn. of vinylmagnesium bromide, stirring (overnight, room temp.); removal of solvent, extn. (hot hexane), removal of solvent, decompn. on futher purification;
References:
Jackson, Logan A.;Allen, Christopher W. [Journal of the Chemical Society, Dalton Transactions,1989,p. 2423 - 2428]
917-64-6
149 suppliers
$45.00/10ml
1004-35-9
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877-07-6
5 suppliers
$156.00/250MG
74-83-9
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$28.30/1ML
5314-85-2
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16445-02-6
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16444-94-3
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877-07-6
5 suppliers
$156.00/250MG