Boronic acid, B-[(1E)-2-(3-thienyl)ethenyl]- synthesis
- Product Name:Boronic acid, B-[(1E)-2-(3-thienyl)ethenyl]-
- CAS Number:1155956-91-4
- Molecular formula:C6H7BO2S
- Molecular Weight:153.99
6165-69-1
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Yield:1155956-91-4 67%
Reaction Conditions:
with potassium phosphate;dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2;water in tetrahydrofuran at 90; for 4 h;Inert atmosphere;Sealed tube;Microwave irradiation;Suzuki-Miyaura Coupling;
References:
Muir, Calum W.;Vantourout, Julien C.;Isidro-Llobet, Albert;Macdonald, Simon J. F.;Watson, Allan J. B. [Organic Letters,2015,vol. 17,# 24,p. 6030 - 6033] Location in patent:supporting information