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ChemicalBook CAS DataBase List BROMINE-1,4-DIOXANE COMPLEX
15481-39-7

BROMINE-1,4-DIOXANE COMPLEX synthesis

2synthesis methods
A 1:1 complex between 1,4-dioxane and bromine has been prepared and isolated on a 2 mol scale by the addition of bromine to 1,4-dioxane. Bromine-1,4-dioxane complex has also been prepared in situ.
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Yield:15481-39-7 57%

Reaction Conditions:

with bromine at 0 - 23; for 3 h;

References:

Salahi, Farbod;Purohit, Vatsal;Ferraudi, Guillermo;Stauffacher, Cynthia;Wiest, Olaf;Helquist, Paul [Organic Letters,2018,vol. 20,# 9,p. 2547 - 2550] Location in patent:supporting information

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