Butanamide, 3-amino- synthesis
- Product Name:Butanamide, 3-amino-
- CAS Number:5959-32-0
- Molecular formula:C4H10N2O
- Molecular Weight:102.135
15846-25-0
33 suppliers
inquiry
5959-32-0
3 suppliers
inquiry
Yield:5959-32-0 97.8%
Reaction Conditions:
with hydrogen in methanol at 40; under 750.075 Torr;Autoclave;
Steps:
1.2; 2.2 Example 1
(2) Add 100 mL of methanol to a 250 mL autoclave with mechanical stirring.3-Aminocrotonamide (8.16 g, 0.08 mol) represented by formula (II-1)Raney nickel 0.4g, access H2, maintain pressure 0.1MPa,Reaction at 40 °C, after complete detection by liquid chromatography,The catalyst was removed by filtration, and the solvent was distilled off under reduced pressure to obtain the formula (III-1).3-aminobutenamide 7.98 g, purity 98.0% by liquid chromatographyYield 97.8%. Liquid chromatography detection conditions: C18 column,The mobile phase volume was: acetonitrile: 0.05% (v:v) aqueous formic acid = 60:40.
References:
CN107501120,2017,A Location in patent:Paragraph 0021; 0023; 0024; 0027; 0028
666844-59-3
0 suppliers
inquiry
5959-32-0
3 suppliers
inquiry
10234-76-1
6 suppliers
inquiry
5959-32-0
3 suppliers
inquiry
10544-63-5
60 suppliers
inquiry
5959-32-0
3 suppliers
inquiry
107-93-7
329 suppliers
$11.19/100G
5959-32-0
3 suppliers
inquiry