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73037-90-8

CHEMBRDG-BB 4004366 synthesis

3synthesis methods
-

Yield:73037-90-8 75%

Reaction Conditions:

Stage #1: 4-chlorobenzaldehyde;propan-1-ol-3-aminewith titanium(IV) isopropylate in tetrahydrofuran at 20; for 8 h;
Stage #2: with sodium tetrahydroborate in tetrahydrofuran;ethanol at 20; for 7 h;

References:

Kumpaty, Hephzibah J.;Bhattacharyya, Sukanta;Rehr, Erik W.;Gonzalez, Amelia M. [Synthesis,2003,# 14,p. 2206 - 2210]

CHEMBRDG-BB 4004366 Related Search: