CHEMBRDG-BB 6423830 synthesis

4synthesis methods

Product Name:CHEMBRDG-BB 6423830
CAS Number:83490-13-5
Molecular formula:C13H10N2O2
Molecular Weight:226.23

98-01-1 Synthesis

98-01-1
471 suppliers
$22.00/25g

58-08-2 Synthesis

58-08-2
10 suppliers
$12.00/1mg

83490-13-5
11 suppliers
$65.00/100mg

Yield:83490-13-5 75%

Reaction Conditions:

Stage #1: 3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dionewith pyridine;palladium diacetate;copper(II) acetate monohydrate in 1,4-dioxane at 20; for 0.166667 h;Inert atmosphere;
Stage #2: furfural in 1,4-dioxane at 120; for 20 h;Inert atmosphere;

References:

Xi, Peihua;Yang, Fan;Qin, Song;Zhao, Dongbing;Lan, Jingbo;Gao, Ge;Hu, Changwei;You, Jingsong [Journal of the American Chemical Society,2010,vol. 132,# 6,p. 1822 - 1824] Location in patent:supporting information; experimental part

98-01-1 Synthesis

98-01-1
471 suppliers
$22.00/25g

1632-83-3 Synthesis