chlorozinc(1+),ethynyl(trimethyl)silane synthesis
- Product Name:chlorozinc(1+),ethynyl(trimethyl)silane
- CAS Number:78389-87-4
- Molecular formula:C5H10ClSiZn
- Molecular Weight:199.0614
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Yield:-
Reaction Conditions:
with n-butyllithium in tetrahydrofuran;hexane;BuLi in hexane was added at -60°C under N2 to a stirred soln. of Me3SiCCH in THF, after 10 min a soln. of ZnCl2 in THF was added, mixt. was stirred for addnl. 15 min at -20°C; not isolated from the soln., used directly for further reactions;
References:
Ruitenberg, K.;Westmijze, H.;Kleijn, H.;Vermeer, P. [Journal of Organometallic Chemistry,1984,vol. 277,# 2,p. 227 - 234]