Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
logo
Inquriy
Try our best to find the right business for you.
Messages
Do not miss inquiry messages Please log in to view all inquiry messages.
My chemicalbook

Welcome back!

Structured search
18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List Chlorsulfuron
64902-72-3

Chlorsulfuron synthesis

2synthesis methods
Chlorsulfuron is produced commercially through a multi-step synthesis that centres on the use of o-chlorobenzenesulfonamide as a key intermediate. The process begins with the preparation of this sulfonamide, which is then reacted with a triazine derivative, specifically, 4-methoxy-6-methyl-1,3,5-triazin-2-amine. This reaction forms a sulfonylurea linkage, resulting in the active compound, 2-chloro-N-[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)carbamoyl]benzenesulfonamide. The synthesis is carried out under controlled conditions to ensure high yield and purity, often using organic solvents and catalysts to facilitate the coupling reaction.
6961-82-6 Synthesis
o-Chlorobenzenesulfonamide

6961-82-6
172 suppliers
$7.00/25g

Chlorsulfuron

64902-72-3
0 suppliers
$65.00/250mg

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1,4-diaza-bicyclo[2.2.2]octane / toluene / 20 h / 20 - 100 °C
2: toluene / 8 h / 70 °C

References:

Hua, Xue-Wen;Chen, Ming-Gui;Zhou, Shaa;Zhang, Dong-Kai;Liu, Ming;Zhou, Sha;Liu, Jing-Bo;Lei, Kang;Song, Hai-Bin;Li, Yong-Hong;Gu, Yu-Cheng;Li, Zheng-Ming [RSC Advances,2016,vol. 6,# 27,p. 23038 - 23047]

FullText

2-Chlorobenzenesulfonyl isocyanate

64900-65-8
49 suppliers
$70.00/500 mg

1668-54-8 Synthesis
2-Amino-4-methoxy-6-methyl-1,3,5-triazine

1668-54-8
241 suppliers
$8.00/10g

Chlorsulfuron

64902-72-3
0 suppliers
$65.00/250mg

References

Chlorsulfuron Related Search:

Methylparaben 4-Methoxyphenylacetone 1,5-Diphenylcarbazide Chlorpropamide 4-Methoxy-N,6-dimethyl-1,3,5-triazin-2-amine