Cilofexor synthesis
- Product Name:Cilofexor
- CAS Number:1418274-28-8
- Molecular formula:C28H22Cl3N3O5
- Molecular Weight:586.85
1418274-31-3
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1418274-28-8
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: isopropylmagnesium bromide / tetrahydrofuran / 1 h / 40 °C / Inert atmosphere
1.2: 16 h / -30 - 20 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / dichloromethane / 16 h / 20 - 30 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 50 °C
4.1: lithium hydroxide monohydrate / tetrahydrofuran; ethanol; water / 16 h / 20 - 30 °C
References:
CN115215853,2022,A
1268245-50-6
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1418274-28-8
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855403-42-8
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$12.00/100mg
1418274-28-8
64 suppliers
$34.00/1mg