cyclohexanol, 2-(1-pyrrolidinyl)-, (1R,2R)- synthesis
- Product Name:cyclohexanol, 2-(1-pyrrolidinyl)-, (1R,2R)-
- CAS Number:247024-86-8
- Molecular formula:C10H19NO
- Molecular Weight:169.26
123-75-1
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Yield:29 % ee
Reaction Conditions:
with soyafibe S-DN in water;toluene at 40; for 144 h;
Steps:
4.4. General Procedure for Catalytic Amination of Epoxide with Amine at the 0.5 mL Scale
General procedure: A mixture of epoxide (0.49 mmol), amine (0.60 mmol), and a catalyst (100 mg) in toluene (0.42 mL)and water (0.02 mL) was shaken at 40 C for the specified time. After removing the catalyst by filtration,the filtrate was analyzed by GC and HPLC. The conversion was calculated as follows, using the conceptof eective carbon number (ECN) [23]:
References:
Asano, Tatsuhiro;Kurata, Hiroyuki;Takeuchi, Yuki;Tsuzaki, Kazuya;Wada, Koichi [Molecules,2020,vol. 25,# 14]