CYCLOHEXANONE PHENYLHYDRAZONE synthesis
- Product Name:CYCLOHEXANONE PHENYLHYDRAZONE
- CAS Number:946-82-7
- Molecular formula:C12H16N2
- Molecular Weight:188.27
108-94-1
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$12.00/50g
100-63-0
388 suppliers
$10.00/1g
946-82-7
13 suppliers
$60.00/500mg
Yield:946-82-7 90%
Reaction Conditions:
with 1-deoxy-1-(methylamino)-D-glucitol in ethanol;water at 20; for 0.416667 h;Green chemistry;
Steps:
General procedure for synthesis of hydrazones
General procedure: Meglumine (0.15 mmol) was added to a mixture of carbonyl compound (1 mmol) andhydrazine (1 mmol) in water-ethanol (1:1, 4 ml). The reaction mixture was stirred at room temperature and monitored by thin-layer chromatography (TLC). After completion of the reaction, water (5 ml) and ethyl acetate (5 ml) were added and the product was extracted with ethyl acetate. The organic phase was dried over anhydrous Na2SO4, and the solvent was removed under vacuum. The crude product was then purified by column chromatography or recrystallized (petroleum ether-EtOAc).
References:
Zhang, Mo;Shang, Ze-Ren;Li, Xiao-Tang;Zhang, Jia-Nan;Wang, Yong;Li, Kang;Li, Yang-Yang;Zhang, Zhan-Hui [Synthetic Communications,2017,vol. 47,# 2,p. 178 - 187]
59-88-1
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$15.00/10g
108-94-1
577 suppliers
$12.00/50g
946-82-7
13 suppliers
$60.00/500mg
4410-13-3
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100-63-0
388 suppliers
$10.00/1g
74-93-1
145 suppliers
$454.02/5MG
946-82-7
13 suppliers
$60.00/500mg