ChemicalBook CAS DataBase List Cyclopentane-1,1-diacetic acid

Cyclopentane-1,1-diacetic acid synthesis

9synthesis methods

Product Name:Cyclopentane-1,1-diacetic acid
CAS Number:16713-66-9
Molecular formula:C9H14O4
Molecular Weight:186.21

4167-77-5
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16713-66-9
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 0.5 h / Inert atmosphere; Cooling
2.2: -3 - 20 °C / Inert atmosphere
3.1: N,N-dimethyl-formamide / 100 °C / Inert atmosphere
4.1: water; sodium hydroxide / ethanol / Inert atmosphere; Reflux

References:

BETA PHARMA CANADA INC;ASTAR BIOTECH LLC;WANG, Zhaoyin;LI, Lianhai WO2013/185202, 2013, A1

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16713-66-9
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References

82683-51-0 Synthesis

82683-51-0
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16713-66-9
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References

5763-53-1
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References

1,1-Cyclopentanedimethanol, 1,1-dimethanesulfonate

62161-65-3
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16713-66-9
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References

Cyclopentane-1,1-diacetic acid Related Search:

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