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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List Dichloromethanesulfenyl chloride
42172-24-7

Dichloromethanesulfenyl chloride synthesis

8synthesis methods
To an ice-cooled dry flask containing 25.0 gm (0.18 mole) of s-trithiane is slowly added dry chlorine gas. As soon as the solid liquefies, the temperature is raised to 10-20°C, and approximately a total of 57.0 gm (0.80 mole) of chlorine gas is absorbed. The product is distilled under reduced pressure to afford 9.9-12.9 gm (46-60%), b.p. 30°C (10 mm Hg).
Preparation of Dichloromethanesulfenyl Chloride
624-92-0 Synthesis
Dimethyl disulfide

624-92-0
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Dichloromethanesulfenyl chloride

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Yield:-

Reaction Conditions:

with chlorine in dichloromethane at -78 - 20;

References:

Block, Eric;Jeon, Hak Rim;Zhang, Shao-Zhong;Dikarev, Evgeny V. [Organic Letters,2004,vol. 6,# 3,p. 437 - 440]

Methanesulfenyl chloride, chloro- (6CI,7CI,8CI,9CI)

26826-80-2
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Dichloromethanesulfenyl chloride

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References
Methane, trichloro[(dichloromethyl)thio]-

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Dichloromethanesulfenyl chloride

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Methane, trichloro[(chloromethyl)thio]-

1454-96-2
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Methane, thiobis[trichloro- (9CI)

60565-85-7
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Dichloromethanesulfenyl chloride

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References
1,3,5-TRITHIANE

291-21-4
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Dichloromethanesulfenyl chloride

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References