DIETHYL DIPHENYLMETHYLAMIDOPHOSPHATE synthesis

2synthesis methods

934-56-5 Synthesis

Yield:57673-92-4 84%

Reaction Conditions:

bis(acetonitrile)(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate in tetrahydrofuran at 60; for 20 h;Phenylation;

References:

Oi, Shuichi;Moro, Mitsutoshi;Fukuhara, Hiroe;Kawanishi, Takanori;Inoue, Yoshio [Tetrahedron Letters,1999,vol. 40,# 52,p. 9259 - 9262]

108-86-1 Synthesis

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