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ChemicalBook CAS DataBase List Dihydrochelirubine
28342-26-9

Dihydrochelirubine synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
2: 28 mg / H2 / Raney Ni / methanol / 4 h / Ambient temperature
3: 1.) HCl, isopentyl nitrite / 1.) AcOH, -5 deg C, 20 min, 2.) RT, 24 h
4: 1.5 mg / NaBH4 / methanol / 0.25 h / Ambient temperature

References:

Konda;Urano;Harigaya [Journal of Heterocyclic Chemistry,1992,vol. 28,# 8,p. 1841 - 1843]