ChemicalBook CAS DataBase List DIIODOSILANE

DIIODOSILANE synthesis

2synthesis methods

Product Name:DIIODOSILANE
CAS Number:13760-02-6
Molecular formula:H2I2Si
Molecular Weight:283.91

Preparative Method of Diiodosilane: phenylsilane and iodine are mixed in a 1:1 molar ratio without solvent at -20 °C in the presence of catalytic amounts of ethyl acetate; fractional distillation removes volatile side products (benzene and HI) and affords the reagent in the form of a colorless oil.

10034-85-2
348 suppliers
$35.00/25g

7440-21-3
228 suppliers
$30.00/100 gm

13760-02-6
53 suppliers
$86.70/5g

13465-72-0
4 suppliers
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13465-84-4
84 suppliers
$73.00/2g

13598-42-0
3 suppliers
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Yield:-

Reaction Conditions:

aluminium(III) iodide in neat (no solvent)reaction at 80°C and 500 Torr;; fractional distillation and condensation;;

References:

Maddock, A. G.;Reid, C.;Emeleus, H. J. [Nature,1939,vol. 144,p. 328 - 328]

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775-12-2 Synthesis

775-12-2
218 suppliers
$10.00/1g

10034-85-2
348 suppliers
$35.00/25g

13760-02-6
53 suppliers
$86.70/5g

References

DIIODOSILANE Related Search:

Sulfur hexafluoride Dichloromethylsilane

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