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ChemicalBook CAS DataBase List (-)-Dipivaloyl-L-tartaric Acid
65259-81-6

(-)-Dipivaloyl-L-tartaric Acid synthesis

1synthesis methods
Preparative Method of (2R,3R)-Dipivaloyltartaric Acid: hydrolysis of the corresponding anhydride obtained by heating (2R,3R)-tartaric acid and pivaloyl chloride at 120-140 °C for 4 h.[1] Drying: over P2O5 in vacuo, controlled by 1H NMR and optical rotations.
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Yield:-

References:

Davenport, Kenneth G.;Mao, David T.;Richmond, Cliff M.;Bergbreiter, David E.;Newcomb, Martin [Journal of Chemical Research, Miniprint,1984,# 5,p. 1518 - 1530]