DODECANE,3-METHYL- synthesis
- Product Name:DODECANE,3-METHYL-
- CAS Number:17312-57-1
- Molecular formula:C13H28
- Molecular Weight:184.36
463-18-3
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15366-08-2
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Yield: 72 %Chromat.
Reaction Conditions:
Stage #1:s-butylmagnesium chloride with buta-1,3-diene;copper(l) chloride in tetrahydrofuran at 50; for 0.166667 h;
Stage #2:n-nonyl fluoride in tetrahydrofuran at 50; for 24 h;regioselective reaction;
References:
Iwasaki, Takanori;Shimizu, Ryohei;Imanishi, Reiko;Kuniyasu, Hitoshi;Kambe, Nobuaki [Angewandte Chemie - International Edition,2015,vol. 54,# 32,p. 9347 - 9350][Angew. Chem.,2015,vol. 127,# 32,p. 9479 - 9482,4] Location in patent:supporting information
71138-64-2
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17312-57-1
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693-58-3
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15366-08-2
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693-58-3
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15366-08-2
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106-99-0
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925-52-0
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917-64-6
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1534-27-6
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