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ChemicalBook CAS DataBase List E-2-OCTADECENAL

E-2-OCTADECENAL synthesis

11synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 73 percent / lithium diisopropylamide, hexamethylphosphortriamide / tetrahydrofuran / -78 °C
2: tetrafluoroboric acid (50percent) / CH2Cl2; H2O / 7 h / Heating
3: 90 percent / NaHCO3 / tetrahydrofuran; H2O / 4 h / Heating

References:

Pohmakotr, Manat;Pisutjaroenpong, Somchai [Tetrahedron Letters,1985,vol. 26,# 30,p. 3613 - 3616]

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