ethyl 2-(6-aminopyridin-3-yl)acetate synthesis

4synthesis methods

Product Name:ethyl 2-(6-aminopyridin-3-yl)acetate
CAS Number:1174229-72-1
Molecular formula:C9H12N2O2
Molecular Weight:180.2

52092-47-4 Synthesis

52092-47-4
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1174229-72-1
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$123.00/100mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C
1.2: 4 h / 80 °C
2.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C
3.1: hydrogen; palladium 10% on activated carbon / methanol / 2 h / 20 °C

References:

MERCK SHARP & DOHME CORP.;DONG, Shuzhi;PASTERNAK, Alex;SUZUKI, Takao;GU, Xin;FU, Qinghong;JIANG, Jinlong;DING, Fa-Xiang;TANG, Haifeng;DEJESUS, Reynalda K. WO2015/96035, 2015, A1

FullText

Propanedioic acid, 2-(6-nitro-3-pyridinyl)-, 1-(1,1-dimethylethyl) 3-ethyl ester

1333509-17-3
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1174229-72-1
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$123.00/100mg

References

39856-50-3 Synthesis

39856-50-3
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1174229-72-1
41 suppliers
$123.00/100mg

References

1072-98-6
692 suppliers
$5.00/1g

1174229-72-1
41 suppliers
$123.00/100mg

References