ETHYL (3-NITRO-2-OXO-1,2-DIHYDROPYRIDYL)ACETATE synthesis
- Product Name:ETHYL (3-NITRO-2-OXO-1,2-DIHYDROPYRIDYL)ACETATE
- CAS Number:147283-76-9
- Molecular formula:C9H10N2O5
- Molecular Weight:226.19
6332-56-5
358 suppliers
$10.00/5g
105-36-2
355 suppliers
$5.00/5G
147283-76-9
13 suppliers
$45.00/50mg
Yield:147283-76-9 98%
Reaction Conditions:
Stage #1: 2-hydroxy-3-nitropyridinewith sodium hydride in tetrahydrofuran; for 0.5 h;
Stage #2: ethyl bromoacetate in tetrahydrofuran at 55; for 36 h;Further stages.;
References:
Karis, N. David;Loughlin, Wendy A.;Jenkins, Ian D. [Tetrahedron,2007,vol. 63,# 50,p. 12303 - 12309]
6332-56-5
358 suppliers
$10.00/5g
623-48-3
0 suppliers
$58.89/5g
147283-76-9
13 suppliers
$45.00/50mg
6332-56-5
358 suppliers
$10.00/5g
105-36-2
355 suppliers
$5.00/5G
147283-76-9
13 suppliers
$45.00/50mg
6332-56-5
358 suppliers
$10.00/5g
623-48-3
0 suppliers
$58.89/5g
147283-76-9
13 suppliers
$45.00/50mg