ETHYL 3-OXOBICYCLO[3.1.0]HEXANE-6-CARBOXYLATE synthesis

3synthesis methods

Product Name:ETHYL 3-OXOBICYCLO[3.1.0]HEXANE-6-CARBOXYLATE
CAS Number:1515923-85-9
Molecular formula:C9H12O3
Molecular Weight:168.19

14320-38-8 Synthesis

14320-38-8
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ETHYL 3-OXOBICYCLO[3.1.0]HEXANE-6-CARBOXYLATE

1515923-85-9
19 suppliers
$265.00/100mg

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 1H-imidazole / N,N-dimethyl-formamide / 14 h / 20 °C
2: dirhodium tetraacetate / dichloromethane / 14 h / 20 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 - 50 °C
4: Dess-Martin periodane / dichloromethane / 15 h / 20 °C

References:

WO2014/9295,2014,A1

tert-butyl(cyclopent-3-enyloxy)dimethylsilane

68845-72-7
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1515923-85-9
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References

ethyl 3-[(tert-butyldimethylsilyl)oxy]bicyclo [3.1.0]hexane-6-carboxylate

1515923-83-7
1 suppliers
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1515923-85-9
19 suppliers
$265.00/100mg

References

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