Ethyl 4,6-dichloro-1H-indole-2-carboxylate synthesis
- Product Name:Ethyl 4,6-dichloro-1H-indole-2-carboxylate
- CAS Number:53995-82-7
- Molecular formula:C11H9Cl2NO2
- Molecular Weight:258.1
554-00-7
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53995-82-7
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: hydrogenchloride; sodium nitrite / water / 0.75 h / -3 °C
1.2: 0 °C
1.3: 2 h / 0 °C / Reflux
2.1: poly phosphoric acid / 1,2-dichloro-ethane / 12 h / Reflux
References:
Iioka, Ryoya;Yorozu, Kohei;Sakai, Yoko;Kawai, Rika;Hatae, Noriyuki;Takashima, Katsuki;Tanabe, Genzoh;Wasada, Hiroaki;Yoshimatsu, Mitsuhiro [European Journal of Organic Chemistry,2021,vol. 2021,# 10,p. 1553 - 1558]
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103855-01-2
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1000210-73-0
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53995-82-7
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617-35-6
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63352-99-8
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53995-82-7
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626-43-7
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53995-82-7
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