ChemicalBook CAS DataBase List Ethyl 4-Nitrobutanoate

Ethyl 4-Nitrobutanoate synthesis

4synthesis methods

Product Name:Ethyl 4-Nitrobutanoate
CAS Number:2832-16-8
Molecular formula:C6H11NO4
Molecular Weight:161.16

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Yield: 98%

Reaction Conditions:

hydrotalcite structure integrating fluoride ions in acetonitrile at 25; for 2 h;Conversion of starting material;Michael Condensation;

Steps:

3.k
The catalyst obtained in example 1 was utilised to catalyse Michael's reactions by global budget/balance: Table 2, hereunder, groups the results observed for different kinds of acceptors and donors. The corresponding reactions (a) to (k) were achieved through reaction at a temperature of 25° C., under agitation and in 5 ml of dry acetonitril, 1 millimole of an acceptor like compound and 1 millimole of a donor like compound, in the presence of 0.1 g of ‘HDT-F’ catalyst prepared in example 1.

References:

COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH (C.S.I.R) US2005/250963, 2005, A1 Location in patent:Page/Page column 5; 7

75-52-5
4 suppliers
$31.19/100g

140-88-5
512 suppliers
$12.00/100ml

2832-16-8
17 suppliers
inquiry