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ChemicalBook CAS DataBase List FMOC-HOMOCYS(TRT)-OH
167015-23-8

FMOC-HOMOCYS(TRT)-OH synthesis

4synthesis methods
82911-69-1 Synthesis
N-(9-Fluorenylmethoxycarbonyloxy)succinimide

82911-69-1
645 suppliers
$7.00/25g

-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: Na2CO3 / H2O / 12 h / 25 °C
1.2: H2O; dioxane / 4 h / 25 °C
1.3: 90 percent / citric acid / H2O; dioxane / pH 4
2.1: 85 percent / dithiothreitol / dimethylformamide; H2O / 4 h / 50 °C
3.1: 60 percent / trifluoroacetic acid / CH2Cl2 / 6 h / 25 °C

References:

Jiang, Luyong;Burgess, Kevin [Tetrahedron,2002,vol. 58,# 43,p. 8743 - 8750]

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