FURAN-2-YL(THIOPHEN-3-YL)METHANOL synthesis
- Product Name:FURAN-2-YL(THIOPHEN-3-YL)METHANOL
- CAS Number:136260-85-0
- Molecular formula:C9H8O2S
- Molecular Weight:180.22
110-00-9
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$10.00/25g
498-62-4
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$5.00/1g
136260-85-0
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$437.00/1g
Yield:136260-85-0 86.6%
Reaction Conditions:
Stage #1: furanwith n-butyllithium in tetrahydrofuran;hexane at -78 - 0;Inert atmosphere;
Stage #2: 3-thiophene carboxaldehyde in tetrahydrofuran;hexane at -78 - 0;Inert atmosphere;
Stage #3: with water;ammonium chloride in tetrahydrofuran;hexane at 0;Inert atmosphere;
References:
Singh, Vishwakarma;Singh, Vikrant [Synthetic Communications,2010,vol. 40,# 9,p. 1280 - 1291] Location in patent:experimental part