Hydrazine, 1-Methyl-2-phenyl-, hydrochloride (1:1) synthesis
- Product Name:Hydrazine, 1-Methyl-2-phenyl-, hydrochloride (1:1)
- CAS Number:92304-54-6
- Molecular formula:C7H11ClN2
- Molecular Weight:158.6286
108-86-1
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: copper(l) iodide; N-(2,6-dimethylphenyl)-6-hydroxypicolinamide; potassium carbonate / dimethyl sulfoxide / 8 h / 75 °C / Inert atmosphere
2: chloro-trimethyl-silane / methanol / 3 h / 4 - 20 °C / Inert atmosphere
References:
Schmidt, Michael A. [Journal of Organic Chemistry,2022,vol. 87,# 4,p. 1941 - 1960]