Hydrazine, (4-biphenylyl)-, hydrochloride synthesis
- Product Name:Hydrazine, (4-biphenylyl)-, hydrochloride
- CAS Number:63543-02-2
- Molecular formula:C12H12N2.ClH
- Molecular Weight:0
92-66-0
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63543-02-2
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Yield:63543-02-2 84%
Reaction Conditions:
Stage #1: 4-bromo-1,1'-biphenylwith potassium phosphate;copper(l) iodide;N,N′-bis(2,6-dimethylphenyl)oxalamide;cetyltrimethylammonim bromide in water at 80; for 0.25 h;Schlenk technique;Inert atmosphere;Sealed tube;
Stage #2: with hydrazine hydrate in water at 80;Inert atmosphere;Schlenk technique;Sealed tube;
Stage #3: with hydrogenchloride in water; pH=3 - 4;Inert atmosphere;Schlenk technique;Sealed tube;
References:
Kumar, Siripuram Vijay;Ma, Dawei [Chinese Journal of Chemistry,2018,vol. 36,# 11,p. 1003 - 1006] Location in patent:supporting information
92-67-1
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$19.89/1g
63543-02-2
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