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ChemicalBook CAS DataBase List Hydroxy-2-phenylpropyl CarbaMate
25451-53-0

Hydroxy-2-phenylpropyl CarbaMate synthesis

3synthesis methods
-

Yield:25451-53-0 63%

Reaction Conditions:

Stage #1: 2-phenylpropane-1, 3-diol;1,1'-carbonyldiimidazole in tetrahydrofuran at 20; for 1 h;
Stage #2: with ammonia in tetrahydrofuran at -48; for 3 h;

References:

Thompson, Charles D.;Gulden, Pamela H.;Macdonald, Timothy L. [Chemical Research in Toxicology,1997,vol. 10,# 4,p. 457 - 462]