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ChemicalBook CAS DataBase List Hydroxylamine, O-[(1,1-dimethylethoxy)carbonyl]-
86031-24-5

Hydroxylamine, O-[(1,1-dimethylethoxy)carbonyl]- synthesis

2synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
863 suppliers
$13.50/25G

36016-38-3 Synthesis
tert-Butyl N-hydroxycarbamate

36016-38-3
370 suppliers
$6.00/5g

Hydroxylamine,  O-[(1,1-dimethylethoxy)carbonyl]-

86031-24-5
5 suppliers
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Yield:36016-38-3 72%

Reaction Conditions:

with sodium hydroxide;hydroxylamine hydrochloride in 1,4-dioxane; for 22 h;

References:

Baldwin, Jack E.;Adlington, Robert M.;Mellor, Lisa C. [Tetrahedron,1994,vol. 50,# 17,p. 5049 - 5066]