IMidazo[1,2-a]pyridine, 8-broMo-3-Methyl- synthesis

1synthesis methods

Product Name:IMidazo[1,2-a]pyridine, 8-broMo-3-Methyl-
CAS Number:1288990-82-8
Molecular formula:C8H7BrN2
Molecular Weight:211.06

149489-04-3 Synthesis

CARBAMIC ACID, (3-BROMO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER

149489-04-3
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IMidazo[1,2-a]pyridine, 8-broMo-3-Methyl-

1288990-82-8
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
2: silver trifluoromethanesulfonate / acetonitrile / 96 h / 85 °C / Inert atmosphere

References:

Chioua, Mourad;Soriano, Elena;Infantes, Lourdes;Jimeno, M. Luisa;Marco-Contelles, Jose;Samadi, Abdelouahid [European Journal of Organic Chemistry,2013,# 1,p. 35 - 39]

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