Linzagolix synthesis
- Product Name:Linzagolix
- CAS Number:935283-04-8
- Molecular formula:C22H15F3N2O7S
- Molecular Weight:508.42
773871-99-1
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$60.00/50mg
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: hydrogenchloride / toluene; water / 5 h / 38 - 43 °C
2: sodium hydroxide; tetrabutylammomium bromide / toluene; water / 4 h / 60 - 63 °C
3: acetic acid; nitric acid / 2 h / 59 - 62 °C
4: hydrogen / ethyl acetate / 4 h / 20 °C
5: triethylamine / tetrahydrofuran / 24 h / 20 °C
6: lithium hydroxide / tetrahydrofuran; methanol; water / 1.5 h / 11 - 13 °C
References:
CD: Kissei Pharmaceutical Co., Ltd.;Aiuchi Takayuki;Kasai Kiyoshi;Bei Kubo Shigeru;Ono Kosuke;Sonehara Jun'ichi;Kobayashi Makoto JP6268093, 2018, B2
187543-87-9
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1073435-67-2
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1073435-69-4
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1073435-71-8
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935283-04-8
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