LMK-235 synthesis
- Product Name:LMK-235
- CAS Number:1418033-25-6
- Molecular formula:C15H22N2O4
- Molecular Weight:294.35
78277-26-6
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1418033-25-6
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Yield:-
Steps:
Multi-step reaction with 7 steps
1: triethylamine / acetonitrile / Reflux
2: hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 2 h / 20 °C / 750.08 Torr
3: thionyl chloride / dichloromethane / 2 h / Reflux
4: pyridine / dichloromethane / 18 h / 20 °C
5: methylhydrazine / dichloromethane / 2 h / -10 °C
6: 1,2-dichloro-ethane; dmap / dichloromethane / 24 h / 20 °C
7: hydrogen; palladium 10% on activated carbon / tetrahydrofuran / 4 h / 20 °C / 750.08 Torr
References:
Marek, Linda;Hamacher, Alexandra;Hansen, Finn K.;Kuna, Krystina;Gohlke, Holger;Kassack, Matthias U.;Kurz, Thomas [Journal of Medicinal Chemistry,2013,vol. 56,# 2,p. 427 - 436]
![Hexanoic acid, 6-[(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)oxy]-](/CAS/20210305/GIF/1101114-27-5.gif)
1101114-27-5
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1418033-25-6
111 suppliers
$29.00/1mg
1418033-03-0
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1418033-25-6
111 suppliers
$29.00/1mg