METHYL-(2-METHYL-THIAZOL-4-YLMETHYL)-AMINE synthesis
- Product Name:METHYL-(2-METHYL-THIAZOL-4-YLMETHYL)-AMINE
- CAS Number:144163-81-5
- Molecular formula:C6H10N2S
- Molecular Weight:142.22
39238-07-8
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144163-81-5
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Yield:144163-81-5 99%
Reaction Conditions:
at 25; for 1 h;
Steps:
408.A N-methyl(2-methyl-1,3-thiazol-4-yl)methanamine
2-Methyl-4-(chloromethyl)thiazole (2.94 g, CASNo.39238-07-8) was dissolved in 40% methylamine (39 mL, 25 equivalents) at 25° C. for 1 h. The mixture was evaporated and purified using 10% methanol/dichloromethane with 0.5% NH4OH to give 2.83 g (99%) of the amine.
References:
US2005/131042,2005,A1 Location in patent:Page/Page column 114
77470-53-2
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74-89-5
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144163-81-5
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$45.00/100mg
62-55-5
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534-07-6
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144163-81-5
63 suppliers
$45.00/100mg