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ChemicalBook CAS DataBase List Methyl 3-aminosulfonylthiophene-2-carboxylate

Methyl 3-aminosulfonylthiophene-2-carboxylate synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: NaNO2; glacial acetic acid; aq. HCl / 1 h / 0 °C
1.2: SO2; CuCl2 / acetic acid / 1 h / 0 °C
2.1: aq. NH3 / acetone / 1 h

References:

Bastide;Badon;Cambon;Vega [Pesticide Science,1994,vol. 40,# 4,p. 293 - 297]

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