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METHYL 3-FORMYL-5-METHOXYBENZOATE synthesis

4synthesis methods
13036-02-7 Synthesis
Dimethyl 5-hydroxyisophthalate

13036-02-7
173 suppliers
$6.00/5g

-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 95 percent / K2CO3 / acetone / Heating
2: 83 percent / 85 percent KOH / methanol; tetrahydrofuran / 6 h / Heating
3: 90 percent / BH3*(CH3)2S / tetrahydrofuran / 0 - 60 °C
4: 91 percent / MnO2 / ethyl acetate / 5 h / Heating

References:

Zhao;Thurkauf [Synthetic Communications,2001,vol. 31,# 12,p. 1921 - 1926]