Methyl 4-(Sulfamoylmethyl)benzoate synthesis
- Product Name:Methyl 4-(Sulfamoylmethyl)benzoate
- CAS Number:110654-40-5
- Molecular formula:C9H11NO4S
- Molecular Weight:229.25
2417-72-3
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110654-40-5
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Yield:110654-40-5 71%
Reaction Conditions:
Stage #1: Methyl 4-(bromomethyl)benzoatewith sodium 3-methoxy-3-oxo-propane-1-sulfinate in dimethyl sulfoxide at 20;
Stage #2: with sodium methylate in methanol;dimethyl sulfoxide at 20; for 0.25 h;
Stage #3: with sodium acetate;hydroxylamine-O-sulfonic acid in water at 20; for 20 h;
References:
Baskin, Jeremy M;Wang, Zhaoyin [Tetrahedron Letters,2002,vol. 43,# 47,p. 8479 - 8483]
![BENZOIC ACID, 4-[(CHLOROSULFONYL)METHYL]-, METHYL ESTER](/CAS/GIF/130047-14-2.gif)
130047-14-2
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110654-40-5
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76749-12-7
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110654-40-5
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![4-[(Aminosulfonyl)methyl]benzoic acid](/CAS/GIF/110654-41-6.gif)
![Benzamide, 4-[(aminosulfonyl)methyl]-](/CAS/20210111/GIF/110654-65-4.gif)
110654-65-4
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110654-40-5
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