N-(2-INDOL-3-YLETHYL)-3-PHENYLPROP-2-ENAMIDE synthesis

1synthesis methods

Product Name:N-(2-INDOL-3-YLETHYL)-3-PHENYLPROP-2-ENAMIDE
CAS Number:74582-72-2
Molecular formula:C19H18N2O
Molecular Weight:290.36

61-54-1 Synthesis

61-54-1
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N-(2-INDOL-3-YLETHYL)-3-PHENYLPROP-2-ENAMIDE

74582-72-2
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere
2.1: 3 h / 80 °C / Inert atmosphere
3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
3.2: 4 h / 20 °C / Inert atmosphere

References:

Pakhare, Deepali;Kusurkar, Radhika [New Journal of Chemistry,2016,vol. 40,# 6,p. 5428 - 5431]