N-(2H-1,3-benzodioxol-5-ylmethyl)cyclohexanamine synthesis
- Product Name:N-(2H-1,3-benzodioxol-5-ylmethyl)cyclohexanamine
- CAS Number:227017-79-0
- Molecular formula:C14H19NO2
- Molecular Weight:233.31
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Yield:227017-79-0 82%
Reaction Conditions:
Stage #1: 1,3-benzodioxol-5-ylmethyl amine;cyclohexanone in dichloromethane at 25; for 1.5 h;Molecular sieve;Inert atmosphere;
Stage #2: with sodium tris(acetoxy)borohydride in dichloromethane at 17; for 25 h;Molecular sieve;Inert atmosphere;
References:
Ehmke, Veronika;Quinsaat, Jose Enrico Q.;Rivera-Fuentes, Pablo;Heindl, Cornelia;Freymond, Céline;Rottmann, Matthias;Brun, Reto;Schirmeister, Tanja;Diederich, Fran?ois [Organic and Biomolecular Chemistry,2012,vol. 10,# 30,p. 5764 - 5768] Location in patent:supporting information; experimental part
2620-50-0
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$20.00/10g
108-91-8
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227017-79-0
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