N-Benzyl-1-(5-Methylfuran-2-yl)MethanaMine synthesis
- Product Name:N-Benzyl-1-(5-Methylfuran-2-yl)MethanaMine
- CAS Number:130539-99-0
- Molecular formula:C13H15NO
- Molecular Weight:201.26
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Yield:130539-99-0 97.1%
Reaction Conditions:
with palladium on activated charcoal;hydrogen in ethyl acetate at 70; under 6000.6 Torr; for 1.5 h;Time;
Steps:
2 Example 2.
In a high-pressure reactor with a magnetic stirrer, 7.5 mg of Pd/C, 500 ul of 5-methylfurfural, 20 ml of ethyl acetate, and 490 ul of benzylamine were added successively to shut off the kettle, and the air in the reactor was replaced with hydrogen, and it was ensured that The initial hydrogen pressure of the reaction was 0.8 Mpa. The autoclave was placed in an electric heating jacket, heated to 70° C., and stirred for 1.5 h. After the reaction was analyzed by gas chromatography, the conversion rate of the substrate 5-methylfurfural and benzylamine was 97.47% and 100%, respectively, as calculated by the area normalization method. Intermediate products in the system were obtained.N-(5-methylmercapto)benzylimineAnd target productsN-(5-methylmercapto)benzylamineThe percentages were 0.37% and 97.10%, respectively.
References:
CN107721953,2018,A Location in patent:Paragraph 0022; 0026; 0027; 0039
620-02-0
503 suppliers
$14.14/5gm:
100-46-9
501 suppliers
$5.00/5G
130539-99-0
7 suppliers
$378.00/1g
![Benzenemethanamine, N-[(5-methyl-2-furanyl)methylene]-](/CAS/20210305/GIF/91608-35-4.gif)
91608-35-4
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130539-99-0
7 suppliers
$378.00/1g
620-02-0
503 suppliers
$14.14/5gm:
130539-99-0
7 suppliers
$378.00/1g