N-Boc-2-vinylpyrrolidine synthesis
- Product Name:N-Boc-2-vinylpyrrolidine
- CAS Number:176324-60-0
- Molecular formula:C11H19NO2
- Molecular Weight:197.27
86953-79-9
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176324-60-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: sec.-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether; hexane / 3 h / -78 °C
1.2: 1 h / -78 °C
2.1: n-butyllithium / hexane / 0.5 h / 20 °C / Inert atmosphere
2.2: 0.83 h / -78 - -42 °C
References:
Varela, Ana;Garve, Lennart K. B.;Leonori, Daniele;Aggarwal, Varinder K. [Angewandte Chemie - International Edition,2017,vol. 56,# 8,p. 2127 - 2131][Angew. Chem.,2017,vol. 129,p. 2159 - 2163]
69610-41-9
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1779-49-3
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18922-06-0
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