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ChemicalBook CAS DataBase List N-BUTYLTRICHLOROGERMANE

N-BUTYLTRICHLOROGERMANE synthesis

7synthesis methods
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Yield:4872-26-8 76.3% ,2117-36-4 91.7%

Reaction Conditions:

germanium(II) chloride dioxane in neat (no solvent);mixed, boiled on an oil bath at 320°C for 40 min, temp. of reaction mixture rose during this period from 127°C to 217°C; distilled under vac.;

References:

Pavlov, K. V.;Shvedov, I. P. [Russian Journal of General Chemistry,1994,vol. 64,p. 146 - 146][Zhurnal Obshchei Khimii,1994,vol. 64,p. 160 - 160]