N-hydroxyfuran-2-carboxamide synthesis
- Product Name:N-hydroxyfuran-2-carboxamide
- CAS Number:17698-14-5
- Molecular formula:C5H5NO3
- Molecular Weight:0
88-14-2
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Yield:17698-14-5 89%
Reaction Conditions:
Stage #1: 2-furanoic acidwith 4-methyl-morpholine;2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide in ethyl acetate;acetonitrile at 0; for 0.25 h;
Stage #2: with hydroxylamine hydrochloride in ethyl acetate;acetonitrile;Ultrasonication;
References:
Vasantha, Basavalingappa;Hemantha, Hosahalli P.;Sureshbabu, Vommina V. [Synthesis,2010,# 17,art. no. P05010SS,p. 2990 - 2996] Location in patent:experimental part
527-69-5
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98-01-1
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144223-33-6
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611-13-2
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