Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List N N'-DIPENTYL-3 4 9 10-PERYLENEDICARBOX&
76372-75-3

N N'-DIPENTYL-3 4 9 10-PERYLENEDICARBOX& synthesis

2synthesis methods
-

Yield:-

Reaction Conditions:

in 1H-imidazole at 160; for 1 h;Autoclave;

Steps:

9

10 g (25.5 mmol) of perylene-3,4,9,10-tetracarboxylic dianhydride, 5.2 g (60 mmol) of n-pentylamine and 50 g of imidazol are heated at 160°C for 1 hour in an autoclave. The reaction mixture is then cooled, 200 ml of DMF are added, the mixture is refluxed for 15 minutes and filtered while hot, and the residue is washed with DMF and dried at 60°C/160 mbar, giving 12 g of a red powder

References:

EP977754,2008,B1 Location in patent:Page/Page column 11

N N'-DIPENTYL-3 4 9 10-PERYLENEDICARBOX& Related Search: