N-Phenyl-2-pyridylmethanimine synthesis
- Product Name:N-Phenyl-2-pyridylmethanimine
- CAS Number:7032-25-9
- Molecular formula:C12H10N2
- Molecular Weight:182.22
Yield:7032-25-9 89%
Reaction Conditions:
with CdS-SnS2 composite in toluene at 20; for 6 h;Irradiation;
Steps:
2.4. Photocatalytic performance
General procedure: The photocatalytic cross-coupling of alcohol and amine was performedas model reaction in a 25 mL round-bottomed flask. Generally,alcohol (0.1 mmol), amine (0.1 mmol) and catalyst (50 mg) wereintroduced into the flask with 1.0 mL of n-hexane as reaction solvent.The mixture was stirred in the dark for 15 min to establish adsorptiondesorptionequilibrium before visible light irradiation. Then, irradiationfor 6 h was executed using a 300 W Xe lamp with a 420 nm cut offfilter (PLS-SXE 300 C). The reaction is maintained at room temperatureand the photon flux inside the reactor was measured to be 0.119 Wcm-2.After reaction, the photocatalyst was resolved through centrifugationand the remaining mixture was analyzed by a Shimadzu GC-2010Pluschromatograph fitted with a capillary SH-Rtx-1701 column.
References:
Au, Chak-Tong;Chen, Lang;Guo, Jun-Kang;Shen, Sheng;Tan, Xi-Ping;Yin, Shuang-Feng [Applied Catalysis A: General,2022,vol. 640,art. no. 118660]
4329-81-1
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