N2,N2-Bis(carboxyMethyl) N6-Boc-L-lysine synthesis
- Product Name:N2,N2-Bis(carboxyMethyl) N6-Boc-L-lysine
- CAS Number:752200-93-4
- Molecular formula:C15H26N2O8
- Molecular Weight:362.38
Yield:752200-93-4 65%
Reaction Conditions:
Stage #1: (S)-2-amino-6-(tert-butoxycarbonylamino)hexanoic acid;bromoacetic acidwith sodium hydroxide in water at 0 - 50; for 19 h;Inert atmosphere;
Stage #2: with hydrogenchloride in water at 0 - 5; pH=2;
References:
Brellier, Marie;Barlaam, Bernard;Mioskowski, Charles;Baati, Rachid [Chemistry - A European Journal,2009,vol. 15,# 46,p. 12689 - 12701] Location in patent:experimental part
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752200-93-4
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