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ChemicalBook CAS DataBase List nicotinic anhydride
16837-38-0

nicotinic anhydride synthesis

3synthesis methods
3-pyridine anhydride can be used as an organic reagent.
-

Yield: 97%

Reaction Conditions:

with bis(trichloromethyl) carbonate;N-ethyl-N,N-diisopropylamine in tetrahydrofuran at 0 - 20; for 2 h;

References:

Mukaiyama, Teruaki;Funasaka, Setsuo [Chemistry Letters,2007,vol. 36,# 2,p. 326 - 327]

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